%0 journal article %@ 0884-2914 %A Bachmeier, A., Rathmayr, G.B., Schmauch, J., Schell, N., Stark, A., de Jonge, N., Pippan, R. %D 2019 %J Journal of Materials Research %N 1 %P 58-68 %R doi:10.1557/jmr.2018.185 %T High strength nanocrystalline Cu–Co alloys with high tensile ductility %U https://doi.org/10.1557/jmr.2018.185 1 %X A supersaturated single-phase Cu–26 at.% Co alloy was produced by high-pressure torsion deformation, leading to a nanocrystalline microstructure with a grain size smaller than 100 nm. The nonequilibrium solid solution decomposed during subsequent isothermal annealing. In situ high-energy X-ray diffraction was used to map changes linked to the separating phases, and the development of a nanoscale Cu–Co composite structure was observed. To gain further information about the relationship of the microstructure and the mechanical properties after phase separation, uniaxial tensile tests were conducted on as-deformed and isothermally annealed samples. Based on the in situ diffraction data, different isothermal annealing temperatures were chosen. Miniaturized tensile specimens with a round cross section were tested, and an image-based data evaluation method enabled the evaluation of true stress–strain curves and strain hardening behavior. The main results are as follows: all microstructural states showed high strength and ductility, which was achieved by a combination of strain-hardening and strain-rate hardening.