@misc{boesenberg_characterization_of_2014, author={Boesenberg, U., Pistidda, C., Tolkiehn, M., Busch, N., Saldan, I., Suarez-Alcantara, K., Arendarska, A., Klassen, T., Dornheim, M.}, title={Characterization of metal hydrides by in-situ XRD}, year={2014}, howpublished = {journal article}, doi = {https://doi.org/10.1016/j.ijhydene.2014.02.068}, abstract = {In-situ synchrotron radiation powder X-ray diffraction (SR-PXD) technique is a powerful tool to gain a deeper understanding of reaction mechanisms in crystalline materials. In this paper, the implementation of a new in-situ SR-PXD cell for solid–gas reactions is described in detail. The cell allows performing measurements in a range of pressure which goes from light vacuum (10−2 bar) up to 200 bar and temperatures from room temperature up to 550 °C. The high precision, with which pressure and temperature are measured, enables to estimate the thermodynamic properties of the observed changes in the crystal structure and phase transformations.}, note = {Online available at: \url{https://doi.org/10.1016/j.ijhydene.2014.02.068} (DOI). Boesenberg, U.; Pistidda, C.; Tolkiehn, M.; Busch, N.; Saldan, I.; Suarez-Alcantara, K.; Arendarska, A.; Klassen, T.; Dornheim, M.: Characterization of metal hydrides by in-situ XRD. International Journal of Hydrogen Energy. 2014. vol. 39, no. 18, 9899-9903. DOI: 10.1016/j.ijhydene.2014.02.068}}