%0 journal article %@ 2214-7853 %A Ovodok, E.,Maltanava, H.,Poznyak, S.,Ivanovskaya, M.,Kudlash, A.,Scharnagl, N.,Tedim, J. %D 2017 %J Materials Today: Proceedings %N 11 %P 11526-11533 %R doi:10.1016/j.matpr.2017.09.062 %T Synthesis and characterization of efficient TiO2 mesoporous photocatalysts %U https://doi.org/10.1016/j.matpr.2017.09.062 11 %X Mesoporous TiO2 powder with large surface area and high porosity was prepared via template-free method of heat-stimulated oxidizing,destruction of TiC by HNO3. Anatase crystalline phase of as-prepared and annealed at 200−400 oC titania was confirmed by XRD technique.,Surface nitrate-nitro groups responsible for high adsorption capacity of the TiO2 powders were studied by FTIR spectroscopy. The annealing temperature can be used as a factor for regulation of titania morphology and structural properties. The rise in the annealing temperature higher than the temperature of nitrate-nitro groups decomposition induces the growth of TiO2 crystallites, decreasing porosity and surface area, the drop of adsorption capacity, and improving photocatalytic activity under UV irradiation.